領(lǐng)學(xué)術(shù)科研之先,創(chuàng)食品科技之新
—— 中國食品雜志社
期刊集群
Development of a reversed dispersive based graphene functionalized with multiwalled carbon nanotubes for detection of 2-agonists in pork by high-performance liquid chromatography
來源:食品科學(xué)網(wǎng) 閱讀量: 469 發(fā)表時(shí)間: 2019-09-24
作者: Ying-Wen Qiana,b, Xia Honga,b, Cai-Xia Yuana,b,?, Xin-Kui Zhoua,b, Hai-Ning Hea,b,Dong-Shuai Wanga,b
關(guān)鍵詞: High-performance liquid chromatography,Graphene,Multiwalled carbon nanotube,Ractopamine,Salbutam
摘要:

Areliable and inexpensive pretreatment procedure in the determination of2-agonists in pork was developped. The procedure used a nanocomposite of multiwalled carbon nanotubes (CNTs) functionalized with graphene (rGO) as the reversed dispersive sorbent. It was analyzed after purification by highperformance liquid chromatography, the extraction time and the properties of the nanocomposite were optimized. Under optimized conditions, present method has linear response over concentration range of 0.5–50 ng/mL in pork samples with a satisfactory detection limit close to 0.1 ng/mL. The precisions of the current method (coefficient of variation) are lower than 5%, while recoveries are more than 98.3%. The nanocomposite exhibited high adsorptivity, long-term storage stability, satisfactory anti-interfering activity and high selectivity toward 2-agonists compared with those of rGO and CNTs.

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